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Model PD-501 Portable Multifunctional Measuring Device User�s Guide Brief Introduction: PD-501 portable multifunctional measuring device hereinafter called �the meter�, which is a multifunctional and excellent performance water solution analysis measuring meter. It can be used in lab for high accuracy measurement, which is more suitable for field and online application for environmental protection, water processing project etc. The notable features read as follows: Multifunctional meter can measure the pH, conductivity, ORP (need to extra equip an ORP electrode), mV (need to extra equip a relevant ion electrode) and temperature value. The housing of meter adopts special fold type design, looks good and smart as well as equips with special carrying case, testing electrode and standard buffer solution, make it more convenient for use. Equip with a trinal combination electrode, has automatic temperature compensation function. The meter adopts special LCD, can display 6 functional units. Specifications: Power: DC9V. Electrode: equips along with meter: 201T-F plastic trinal-combination pH electrode; DJS-1 Pt-black conductivity electrode (Constant=1). Optional: DJS-10 Pt-black conductivity electrode (Constant=10); 301Pt-C plastic ORP combination electrode. Dimensions and weight: meter: 95 x 118 x 46mm, weight: 360g Packing: carrying case: 300 x 200 x 90mm. Operation condition: environment temperature 5 to 35!, relevant moisture: d"85%. Main Technical Performance: The technical performance of pH value: Range: 0 to 14 pH. Resolution: 0.01 pH Accuracy: basic error d"�0.01pH �1 digit equipment errord"�0.02pH �1 digit Temperature compensation: 0 to 60!(automatic or manual) Resistance input: e" 1 x 10�12 The technical performance of conductivity value: Measuring range: 0 to 2 x 105&S/cm can be divided to 4 measuring ranges: 0.0 to 199.9&S/cm (test deion water) 0.00 to 19.99mS/cm (test industrial waste water, boiler water and cooling tower water) (a), (b) two measuring ranges equip with DJS-1 Pt-black conductivity electrode which has been already equipped with meter. 0.00 to 1999&S/cm (test drinking water, mineral water) 0.00 to 199.9 mS/cm (test seawater and brine) (c), (d) two measuring ranges equip with DJS-10 Pt-black conductivity electrode (need to extra choose), but can classify (c) measuring range into (b) range, the units is mS/cm. Accuracy: basic error d"�1% F.S �1 digit equipment errord"�1.5% F.S. �1 digit The technical performance of mV value Range: �1500mV Resolution: 1mV Accuracy: d"�0.15% F.S�1digit The technical performance of temperature value Measuring range: 0 to 60! Resolution: 0.1! Accuracy: d"�1! Meter Description and Front Panel Description: LCD Display: The meter adopts 31/2 special used LCD, fold model housing structure, the fold angle can be adjusted freely, not only display measuring value but also display units icon at the same time. Functional Buttons: pH button: Press the button, pH icon will appear on the up right of the LCD that means the meter is in the pH measuring state. mV button: Press the button, mV icon will appear on the middle right of the LCD that means the meter is in the mV measuring state. ! button: Press the button, ! icon will appear on the up left of the LCD, and if insert the temperature probe into it, the meter is in the temperature measuring state. There show the measuring temperature vale on the LCD, if insert the electrode once more, and press the pH button, then the meter is in the automatic temperature compensation for pH measuring state. If only insert the pH electrode, means the meter is in the manual temperature compensation for pH measuring state. As long as twist the temperature button while manual temperature compensation, then the meter will display the value then. &S button: Press this button, &S icon will appear on the bottom right of the LCD that means the meter is in the conductivity measuring state, and the units is &S/cm. mS button: Press the button, mS icon will appear on the middle right of the LCD that means the meter is in the conductivity measuring state, and the units is mS/cm. 1/cm button: Press the button, the 1/cm icon will appear on the end left of the LCD that means the meter is in the conductivity constant state, and twist the �constant� adjustor with the screwdriver, you can adjust the conductivity constant of the meter to meet the electrode�s constant. Adjustor Buttons: Fixed position button: For dissymmetry potential of pH electrode meter�s adjusting while pH measuring. The adjustable range is �1.5pH. Slope button: For compensate the slope error of pH electrode when pH measuring, to meet 2 points calibration of the meter. Temperature button: For temperature adjusting when the meter is in the manual temperature compensation of pH value measuring. (within 0 to 60! range), and the value will be displayed on the LCD. The user should press the ! button and can not insert the temperature sensor at this time. If insert the temperature sensor, the meter is in the temperature measuring state or automatic temperature compensation state. Constant adjustor: Twist the button with the screwdriver while conductivity testing, then the constant of conductivity can be adjusted, and the value will be displayed on the LCD. (user should press the 1/cm button at that time). Socket of Electrode �pH/mV�socket: Be used for connecting with plugs of the pH combination electrode, ORP combination electrode or other combination ion electrodes, the model of electrode plug should be BNC. �conductivity� socket: Be used for connecting with plugs of conductivity electrode, and the model of plug should be Q6-J3.  temperature socket: Be used for connecting with socket of temperature electrode, model of plug should be �3.5 two pins plug, the temperature electrode and pH electrode of this meter are combined together and the �3.5 two pins plug is temperature electrode plug. Power: Press the red button to the left side, then power on and the meter is working, press the button to the right side that indicate power off , or close the display fold on and the meter can also power off automatically. Battery Compartment The battery compartment is in the left up of the meter, and it can be opened with a coin. Measurement Procedure: How to test pH value: Preparation: Open the LCD, and press the ON button to electrify meter. Press the pH button, and the pH icon will appear on the right up of the LCD. Open the pH protection bottle, wash the electrode in distilled water and dry it, and connect the two plugs of electrode with the right �pH/mV� socket separately. Meter�s calibration: Adjust temperature: The meter is in the automatic temperature compensation states when putting the temperature plug of trinal combination electrode into the right side �temperature� socket, and it is unnecessary to adjust the temperature button, just need to press the ! button, and the LCD will display the temperature of standard buffer solution. If use the general pH electrode without temperature plug, then user should test the temperature of solution with thermograph first, and press the ! button, then twist the  temperature� button again, when there shows the relevant temperature value, means the manual temperature compensation finished and press the pH button once more, restore to pH measuring. Fixed position calibration: Immerse electrode into the solution bottle of pH7.00, still it after stirring, and adjust the �fixed position� button, makes the LCD stable display the pH of solution which under this temperature (Details can check the table, such as pHs=7.02 when the temperature is in 20!), if the user want to check the temperature, it will be worked as long as press the ! button. Slope adjusting: Wash electrode with pure water and dry it, and insert it into the bottle of pH 4.00 (or 10.01), still it after stirring. Adjust the  slope button of meter, make the LCD stable display the pH of solution which under this temperature (Detailed data can be checked on the table of bottle, such as pHs=4.00 when the temperature is 20!). Repeat (b) and (c), make the meter shows relative value for this two standard buffer solution, then calibration is finished. Test pH of sample solution: When do high accuracy test, better to do it under the same temperature for testing and calibration, which means the temperature of buffer solution is better the same to temperature of sample solution. Immerse the electrode into the sample solution after washing and drying, and still it after stirring, and take the readings displayed on the LCD. When do general accuracy test, the difference between buffer solution and sample solution is also better not very big, generally d"�15!, at this time if meter keep in the automatic temperature compensation (connected the temperature probe on), as long as place the pH electrode into the sample solution, still it after stirring and take the results then, and the meter can do automatically temperature compensation for the error of pH value which is related to the difference temperature; if the meter is in the manual temperature compensation (without temperature probe or it has not been connected), the temperature should be measured with thermograph, and adjust the temperature button to this temperature value (press ! button), then immerse the electrode into the sample solution for measuring and reading its value. How to test conductivity: Wash and dry the conductivity electrode, insert it into the right side  conductivity socket. Calibration of conductivity constant: Press 1/cm button, adjust the �constant� button with screwdriver, and make the displaying value on the LCD to be the same as the constant of conductivity electrode (Detailed data see the label on the conductivity electrode). For example, the constant of electrode is 10.2 and then make the meter shows 1020 (ignore the decimal point). Choose measuring range according to character of solution, press FS button or mS button, and insert electrode into sample solution, still it after stirring and reading then. How to test ORP or mV: Press mV button, insert the plug of ORP combination electrode or other ion into the right side  pH/mV socket. Wash and dry the electrode, insert it into sample solution, and the meter will display the mV value of ORP electrode or ion electrode as well as show the potential polarity. (The temperature, fixed position and slope button are useless while measuring mV value.) How to test temperature: Press the ! button, insert the temperature plug of trinal combination electrode into right side of  temperature socket, and immerse the electrode into sample solution, then take the results from LCD. Considerations: Considerations on pH measurement: Calibration times for meter depends on sample, electrode performance and accuracy, high accuracy measurement (d"�0.03pH), should calibrate in time and use new fresh standard buffer solution; ordinary accuracy measurement (d"0.1pH), meter can be used for one week or even for longer time once calibration, and the meter must be calibrated when in below situations: The electrode has not been used for a long time or replaced new electrode. After measuring thick acid (pH<2), or thick alkaline (pH>12). After measuring solution contains fluoride or thick organic solution. The solution temperature is much difference with the temperature when calibrating. There are adequate solutions for electrode�s soaking in the front of the protecting bottle. Immerse the head of electrode into it for keeping the activation of glass bulb and junction. When measuring, twist the bottle cap, take electrode out and wash it with distilled water, then it can be used. If find there is thickness or moldy, should wash and replace new soaking solution. How to make up the electrode�s soaking solution: Take 25g analysis KCL and dissolve it into 100mL pure water will be Ok. The electrode should be avoided to be immersed into pure water or protein solution and acidic fluoride solution for a long time, and prevent touching organic silicon oil. When calibrate the meter with known pH value solution, in order to improve accuracy, the pH value of buffer solution should be reliable, the pH value is closer to the sample�s pH value, it will be much better, generally it does not exceed 3 pH, which means user should use pH4.00 buffer solution as slope calibration while measuring acid solution; and use pH10.01 buffer solution as slope calibration while measuring alkaline solution (fixed position calibration always with pH7.00 solution), but pH10.01 solution is easy to go bad, so user should pay attention to its reliability. The sensitive glass bulb in front of the head of pH combination electrode can not be touched with hard thigh for any break or hair will make electrode invalidity. In order to make sure the measurement accuracy, the electrode should be washed with pure water before or after measuring, and it needs to be washed many times with pure water after measuring in thick sample solution for eliminating sample which adhered glass membrane or wash with suitable solvent and washing solvent with clear water. The using life for electrode is one year and user should replace new one in time when it becomes ageing. An electrode being used for a long time or sample solution contains polluted things which easy to pollute sensitive glass bulb to block the junction and make the electrode react slowly, this phenomenon is sensitive gradient reduced and incorrect reading etc. user can adopt the following methods according to different situations: The glass bulb is contaminated and aging: Put the electrode into a 0.1mol/L diluted hydrochloric acid (Preparation: diluted 9ml hydrochloric acid with pure water into 1000ml) for 24h. Rinse it with pure water, then dipped it into the electrode dipping solution for 24 hours. If it is serious passivation, put the end of electrode into 4% HF (hydrofluoric acid) for 3 to 5 seconds, rinsing it with pure water, then dipped it in the electrode dipping solution for 24 hours to make it renew. Washing for glass bulb and junction contamination:(for reference) Inorganic metal oxide diluted hydrochloric acid less than 1M Resin macromolecule matter diluted alcohol/acetone Protein corpuscle deposit acidity enzyme solution Considerations on conductivity measurement: When press FS button, the largest measurement range for meter is 199.9FS/cm(constant of electrode is 1), if meter display  1 (data overflow display), means the conductivity of sample solution has been overflowed measurement range and user should press mS button make the measurement range of meter enlarge 0 to 19.99mS/cm. When using conductivity electrode which constant is 10, measurement range can be enlarged to 0 to 1999FS/cm and 0 to 199.9mS/cm using method is the same to the above, and showed results multiply 10 is the real conductivity of solution. Keeping conductivity electrode clean, user should wash it with pure water after measuring, in order to accuracy measurement, the best way is to wash electrode with sample solution. Due to various variety and consistency solution of conductivity temperature coefficient, temperature compensation of conductivity measurement is complex, so this meter has not adopt temperature compensation circuit and the meter measures the conductivity value is under the current temperature. There are two kinds of conductivity electrode one is bright and the other is Pt black, the purpose for coating with Pt black is to increase the effective area preventing and abating electrode polarity. So use Pt black electrode is the suitable choice. Pt black electrode can be immersing into pure water before using for inert Pt black. If found Pt black electrode incorrectness can immerse it into 10% nitric acid or hydrochloric acid solution for 2 minutes and wash clean with pure water, if this situation have not get better, then the Pt black have to be recoated or buy a new conductivity electrode. The relationship between conductivity and resistance of solution is reciprocal: such as 0.1uS = 1/0.1 = 10M�, user can calculate the resistance value accordingly. The constant for conductivity electrode have been marked (see label on conductivity electrode), but because of temperature is different between consistency of measurement solution and temperature, accuracy of meter and frequency, the constant of conductivity electrode will appear big error, and after using for a period, the electrode�s constant will also to be changed. Therefore, electrode constant for new conductivity electrode and electrode have been using for a long time should be renew calibration. Method for constant of conductivity electrode: use unknown constant electrode to measure known KCl solution of conductivity electrode (adjust the meter�s constant button to 1000, and calculate according to the below formula: J= K/G J: constant for conductivity electrode which is waiting for measurement. K: conductivity of KCl solution under the certain concentration and temperature. G: conductivity results are from KCl solution is measured by unknown constant electrode. For example: Use this meter to test unknown constant DJS-1 Pt-black electrode. Make up mol/L KCl solution, temperature is 25!,see attached table (�N) k=0.0014083S/cm=1.408mS/cm. Press 1/cm button on the meter, adjust constant twist button, make the LCD display 1000. Press mS button, and measured conductivity which in the above KCL solution is G=1.44Ms/cm. According to formula: J=K/G=1.408/1.44=0.978cm-1, then constant for this conductivity electrode is 0.98. Please pay attention to following items when measuring the constant of conductivity electrode. The user should use the present conductivity electrode when measuring. Temperature of KCL solution for electrode constant measurement should be better close to sample solution�s temperature. The consistency of KCL solution for electrode constant measuring should be better close to consistency of sample solution. For example: DJS-1 bright electrode, measuring with 0.001mol/L KCl DJS-1 Pt- black electrode, measuring with 0.01mol/L KCl. DJ S-10 Pt -black electrode, measuring with 0.1mol/L KCl. Other considerations: Keep meter�s clean and dry, especially pay attention to keep connector of meter and electrode clean and dry. Otherwise, it will affect measuring and lead to incorrectness or invalidity. It can wipe with an absorbent cotton dipping absolute alcohol and dry it when the meter is contaminated. When �LOB� icon appears in the middle of LCD, which indicates that the battery is going to fade and please replace a new battery in time. There equip with a small bottle of pure water inside the carrying case is providing for electrode washing during online measuring, please pay attention to replace for avoiding contamination, especially when testing conductivity keeping the pure water inside in the bottle is the most important. What�s Included: 7.1. PD-501 portable functional measuring meter 7.2. 201T-F plastic pH tri-combination electrode 7.3. DJS-1 Pt-black conductivity electrode (constant is 1, Q6-J3 connecter) 7.4. Standard buffer solution pH4.00, 7.00, 10.01 7.5. Pure water for electrode washing 7.6. Screwdriver 7.7. Preparing 9V battery 7.8. Carrying case 7.9. Operation manual Warranty: We warrant this instrument to be free of defects in parts and workmanship for 1 year from date of shipment. Attached electrode is not belong to this warranty range, besides the new one. This warranty does not apply to defects resulting from action of the user such as misuse, improper wiring, operation outside of specification, improper maintenance or repair, or unauthorized modification. Appendix: Concentration of KCl and conductivity value (see table (N)) Approximate Consistency Mol�L-1Conductivity value S�cm-115!18!20!25!35!1 0.1 0.01 0.0010.09212 0.010455 0.0011414 0.00011850.09780 0.011163 0.0012200 0.00012670.10170 0.011644 0.0012737 0.00013220.11131 0.012852 0.0014083 0.00014660.13110 0.015353 0.0016876 0.0001765Table (N) Component of KCl solution (see table (�N)) Approximate Consistency mol�L-1Capacity Consistency KCl g�L-1 solution(in 20! air)1 0.1 0.01 0.00174.2650 7.4365 0.7440 100Ml0.01mol�L-1 Dilute solution for 10 timesTable (�N) How to make up and preserve KCl solution: KCl should adopt excellent pure (GR), and need to be dry out under 220 to 240! for 2 hours, and put it into dryer machine, cool it to room temperature. Conductivity for distilled water or deionize water is < 0.2 x 10-6 S/cm. (25!) Keep solution into a sealed glass container, at room temperature, the valid time is three months. Shanghai San-Xin Instrumentation, Inc. Add: 3/F. Building No.4, No. 471 Guiping Road, Shanghai, China. 200233 Tel: +86-21-63362480 Fax: +86-21-64956880 Website:  HYPERLINK "http://www.shsan-xin.com" www.shsan-xin.com E-mail: wxmab@onlie.sh.cn     PAGE  PAGE 16 PD501 Version5.0 07/06 1set 1pc 1pc 1btl/each 1btl 1pc 1pc 1pc 1book ?cdgklt|���������456@HIRS��DK'�������������θ�����������}wrwrwrwrwrwrwrwrw�}CJaJ CJaJo(5�CJ\�aJo(jCJUaJmHnHu5�CJ$\�aJ5�CJ$\�aJo( CJ$aJo(aJo(CJ,PJaJ,o(5�CJ0\�aJ0 5�CJ\�o( 5�CJ\�o(5�CJ0\�aJ0o( CJ0aJ0o(o(CJo(5�OJPJ\�o(&j5�CJOJPJU\�mHnHu)?cdefgtuvwxyz{|�������������������������������$a$$a$$a$�XWD`�X�x�x%y������������/�U����: � �  ��������������������d�� & F ��������d��^��`��� �d��VD�^� & F�e���^�e`���$d��a$d��$d��a$$a$��: � � � � � � � � � �  � � � � � $ & ( 6 8 | � � � � �   � � � � � �   FN,RT�����FHJXZ���������������������������������������軲�������������������������������� CJaJo(5�CJ\�aJo(CJH*aJo(5�CJ\�aJo(jCJUmHnHuCJPJaJo(CJaJo( CJaJo("j5�CJU\�aJmHnHuD � � � � B j � � J � � \ � <������������������ ��d��VD�^�� & 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